Search results for "C–H···π Interactions"

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Host–guest complexes of conformationally flexible C-hexyl-2-bromoresorcinarene and aromatic N-oxides: solid-state, solution and computational studies

2018

Host–guest complexes of C-hexyl-2-bromoresorcinarene (BrC6) with twelve potential aromatic N-oxide guests were studied using single crystal X-ray diffraction analysis and 1H NMR spectroscopy. In the solid state, of the nine obtained X-ray crystal structures, eight were consistent with the formation of BrC6-N-oxide endo complexes. The lone exception was from the association between 4-phenylpyridine N-oxide and BrC6, in that case the host forms a self-inclusion complex. BrC6, as opposed to more rigid previously studied C-ethyl-2-bromoresorcinarene and C-propyl-2-bromoresorcinarene, undergoes remarkable cavity conformational changes to host different N-oxide guests through C–H···π(host) intera…

Solid-stateCrystal structure010402 general chemistry01 natural scienceslcsh:QD241-441lcsh:Organic chemistryPolarizabilitysupramolekulaarinen kemiaresorcinareneshost–guest chemistryHost–guest chemistrylcsh:Scienceta116Biochemistry Biophysics and Structural BiologyC–H···π Interactions010405 organic chemistryChemistryOrganic Chemistryendo/exo complexationSolution phaseditopic receptors0104 chemical sciencesaromatic N-oxidesChemistryCrystallographyProton NMRPolarlcsh:QSingle crystalBeilstein Journal of Organic Chemistry
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Host-guest complexes of conformationally flexible

2018

Host–guest complexes of C-hexyl-2-bromoresorcinarene (BrC6) with twelve potential aromatic N-oxide guests were studied using single crystal X-ray diffraction analysis and 1H NMR spectroscopy. In the solid state, of the nine obtained X-ray crystal structures, eight were consistent with the formation of BrC6-N-oxide endo complexes. The lone exception was from the association between 4-phenylpyridine N-oxide and BrC6, in that case the host forms a self-inclusion complex. BrC6, as opposed to more rigid previously studied C-ethyl-2-bromoresorcinarene and C-propyl-2-bromoresorcinarene, undergoes remarkable cavity conformational changes to host different N-oxide guests through C–H···π(host) intera…

ChemistryOrganic Chemistryresorcinarenesendo/exo complexationhost–guest chemistryFull Research PaperC–H···π Interactionsditopic receptorsaromatic N-oxidesBeilstein journal of organic chemistry
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